4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

Base Information

Chemical Name:4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside
CAS No.:131283-98-2
Molecular Formula:C₂₄H₃₅NO₁₈
Molecular Weight:625.538
Hs Code.:

Synonyms:4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

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Chemical Property of 4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

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Technology Process of 4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

There total 4 articles about 4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 131283-97-1
4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-2,3-O-isopropylidene-β-D-mannopyranoside

: 131283-98-2
4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

Guidance literature:: With trifluoroacetic acid; In chloroform; water; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(90)80005-N

Reference yield:

: 69649-71-4
2,3,4-tri-O-acetyl-6-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl)-α-D-mannopyranosyl bromide

: 131283-98-2
4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Hg(CN)2 2) 50percent aq. acetic acid / 1) benzene, nitromethane, r.t. 2) 55 deg C, 3 h

2: 72 percent / 0.25M sodium methoxide / methanol / Ambient temperature; overnight

3: 57 percent / trifluoroacetic acid / H₂O; CHCl₃ / 4 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; acetic acid; trifluoroacetic acid; In methanol; chloroform; water;
DOI:10.1016/0008-6215(90)80005-N

Reference yield:

: 126777-62-6
4-nitrophenyl 2,3-O-isopropylidene-β-D-mannopyranoside

: 131283-98-2
4-nitrophenyl O-α-D-mannopyranosyl-(1->6)-O-α-D-mannopyranosyl-(1->6)-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Hg(CN)2 2) 50percent aq. acetic acid / 1) benzene, nitromethane, r.t. 2) 55 deg C, 3 h

2: 72 percent / 0.25M sodium methoxide / methanol / Ambient temperature; overnight

3: 57 percent / trifluoroacetic acid / H₂O; CHCl₃ / 4 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; acetic acid; trifluoroacetic acid; In methanol; chloroform; water;
DOI:10.1016/0008-6215(90)80005-N