dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

Base Information

Chemical Name:dimethyl(phenyl)(propa-1,2-dien-1-yl)silane
CAS No.:75405-41-3
Molecular Formula:C₁₁H₁₄Si
Molecular Weight:174.318
Hs Code.:

Synonyms:dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

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Chemical Property of dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

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Technology Process of dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

There total 6 articles about dimethyl(phenyl)(propa-1,2-dien-1-yl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.6%

: C₁₅H₂₁BNO₂Si^(1-)*H⁽¹⁺⁾

: 75405-41-3
dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

Guidance literature:: C₁₅H₂₁BNO₂Si^(1-)*H⁽¹⁺⁾; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

With water; In dichloromethane; at 20 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol9022529

Reference yield: 96.0%

: 106-96-7
propargyl bromide

: 768-33-2
phenyldimethylsilyl chloride

: 75405-41-3
dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

Guidance literature:: propargyl bromide; With indium; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

phenyldimethylsilyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1016/j.jorganchem.2008.08.028

Reference yield: 89.0%

: 624-65-7
2-propynyl chloride

: 768-33-2
phenyldimethylsilyl chloride

: 75405-41-3
dimethyl(phenyl)(propa-1,2-dien-1-yl)silane

Guidance literature:: phenyldimethylsilyl chloride; With lithium-sodium alloy; In tetrahydrofuran; at 0 ℃; for 5h; Sonication; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

2-propynyl chloride; regioselective reaction; Further stages;
DOI:10.1021/ol301827t