C₂₃H₃₅N₂P

Base Information

• Chemical Name: C₂₃H₃₅N₂P
• CAS No.: 1338599-11-3
• Molecular Formula: C₂₃H₃₅N₂P
• Molecular Weight: 370.518
• Mol file: 1338599-11-3.mol

Synonyms:C₂₃H₃₅N₂P

Chemical Property of C₂₃H₃₅N₂P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₅N₂P

There total 2 articles about C₂₃H₃₅N₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-(2-chloroethyl)-5,6-dimethyl-1H-benzo[d]imidazole (918318-53-3) + dicyclohexylphosphane (829-84-5) → C23H35N2P (1338599-11-3)

Guidance literature:

dicyclohexylphosphane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

1-(2-chloroethyl)-5,6-dimethyl-1H-benzo[d]imidazole; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/om200689r

Reference yield:

5,6-dimethyl-1H-benzo[d]imida-zole (582-60-5) → C23H35N2P (1338599-11-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; potassium carbonate; potassium hydroxide / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 48 h / 20 °C / Inert atmosphere

With n-butyllithium; tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In tetrahydrofuran;

DOI:10.1021/om200689r

Reference yield: 99.0%

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] (12354-84-6,12354-85-7) + C23H35N2P (1338599-11-3) → C33H50Cl2IrN2P

Guidance literature:

In toluene; at 25 ℃; for 12h; Inert atmosphere;

DOI:10.1021/acs.organomet.5b00799

upstream raw materials:

5,6-dimethyl-1H-benzo[d]imida-zole

1-(2-chloroethyl)-5,6-dimethyl-1H-benzo[d]imidazole

dicyclohexylphosphane