(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

Base Information

Chemical Name:(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate
CAS No.:179259-35-9
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

Synonyms:(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

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Chemical Property of (+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

Chemical Property:

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Technology Process of (+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

There total 7 articles about (+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 179259-32-6
(+)-(1S,5R)-3-allyl-2-methyl-5-isopropenylcyclohex-2-enyl acetate

: 179259-35-9
(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

Guidance literature:: With oxygen; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1039/CC9960001369

Reference yield:

: 179259-33-7
(+)-(5S)-3-allyl-2-methyl-5-isopropenylcyclohex-2-enone

: 179259-35-9
(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / LiAlH₄ / diethyl ether / 2 h / -90 °C

2: 95 percent / pyridine; 4-dimethylaminopyridine / CH₂Cl₂ / 8 h / 20 °C

3: 73 percent / CuCl; O₂ / aq. PdCl₂ / dimethylformamide / 24 h / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; oxygen; copper(l) chloride; palladium dichloride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 179259-34-8
(+)-(1S,5R)-3-allyl-2-methyl-5-isopropenylcyclohex-2-enol

: 179259-35-9
(+)-(1S,5R)-5-isopropenyl-3-(2-oxopropyl)-2-methylcyclohex-2-enyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine; 4-dimethylaminopyridine / CH₂Cl₂ / 8 h / 20 °C

2: 73 percent / CuCl; O₂ / aq. PdCl₂ / dimethylformamide / 24 h / 20 °C

With pyridine; dmap; oxygen; copper(l) chloride; palladium dichloride; In dichloromethane; N,N-dimethyl-formamide;