(R)-3-(4-methoxybenzyloxy)tetradecanal

Base Information

Chemical Name:(R)-3-(4-methoxybenzyloxy)tetradecanal
CAS No.:637741-97-0
Molecular Formula:C₂₂H₃₆O₃
Molecular Weight:348.526
Hs Code.:

Synonyms:(R)-3-(4-methoxybenzyloxy)tetradecanal

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Chemical Property of (R)-3-(4-methoxybenzyloxy)tetradecanal

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Technology Process of (R)-3-(4-methoxybenzyloxy)tetradecanal

There total 8 articles about (R)-3-(4-methoxybenzyloxy)tetradecanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 288402-97-1
(R)-1-hydroxy-3-(4-methoxybenzyloxy)tetradecane

: 637741-97-0
(R)-3-(4-methoxybenzyloxy)tetradecanal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 0 ℃;
DOI:10.1039/b305818b

Reference yield: 53.0%

: 1376112-87-6
(R)-3-(4-methoxybenzyloxy)tetradec-1-yne

: 637741-97-0
(R)-3-(4-methoxybenzyloxy)tetradecanal

Guidance literature:: (R)-3-(4-methoxybenzyloxy)tetradec-1-yne; With benzo[1,3,2]dioxaborole; In tetrahydrofuran; at 0 - 70 ℃; for 3.5h; Inert atmosphere;

With sodium acetate; In tetrahydrofuran; water; at 0 ℃; for 0.166667h; pH=7; Inert atmosphere; aq. phosphate buffer;

With dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo300139r

Reference yield:

: 288402-96-0
2-(4-methoxyphenyl)-4-(R)-undecyl-[1,3]dioxane

: 637741-97-0
(R)-3-(4-methoxybenzyloxy)tetradecanal

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / 20 h / 0 °C

2: 84 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 0 °C

With oxalyl dichloride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In hexane; dichloromethane; 2: Swern oxidation;
DOI:10.1039/b305818b