4-mesitylquinazoline

Base Information

Chemical Name:4-mesitylquinazoline
CAS No.:24781-37-1
Molecular Formula:C₁₇H₁₆N₂
Molecular Weight:248.327
Hs Code.:

Synonyms:4-mesitylquinazoline

Suppliers and Price of 4-mesitylquinazoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-mesitylquinazoline

Chemical Property:

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Technology Process of 4-mesitylquinazoline

There total 3 articles about 4-mesitylquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: C₁₇H₂₀N₂

: 24781-37-1
4-mesitylquinazoline

Guidance literature:: With tert.-butylhydroperoxide; iron(II) chloride; In decane; dimethyl sulfoxide; at 25 ℃; for 18h;
DOI:10.1021/acs.joc.7b02943

Reference yield:

: 17583-40-3
2-methylaminobenzonitrile

: 2633-66-1
2-mesitylmagnesium bromide

: 24781-37-1
4-mesitylquinazoline

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 10 - 30 °C / Inert atmosphere

2: iron(II) chloride; tert.-butylhydroperoxide / dimethyl sulfoxide; decane / 18 h / 25 °C

With tert.-butylhydroperoxide; iron(II) chloride; In tetrahydrofuran; decane; dimethyl sulfoxide;
DOI:10.1021/acs.joc.7b02943

Reference yield:

: 24781-37-1
4-mesitylquinazoline

Guidance literature:: 2,4,6-Trimethylphenylmagnesiumbromid, THF, Chinazolin, 1. Siedetemp; 2. Bzl., K3Fe(CN)6, sd. KOH;
DOI:10.1002/hlca.19690520817