4,4-diphenyl-5-methylhexan-1-ol

Base Information

Chemical Name:4,4-diphenyl-5-methylhexan-1-ol
CAS No.:97634-33-8
Molecular Formula:C₁₉H₂₄O
Molecular Weight:268.399
Hs Code.:

Synonyms:4,4-diphenyl-5-methylhexan-1-ol

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Chemical Property of 4,4-diphenyl-5-methylhexan-1-ol

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Technology Process of 4,4-diphenyl-5-methylhexan-1-ol

There total 6 articles about 4,4-diphenyl-5-methylhexan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 97634-32-7
ethyl 4,4-diphenyl-5-methylhexanoate

: 97634-33-8
4,4-diphenyl-5-methylhexan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 5h; Heating;
DOI:10.1021/jm00149a014

Reference yield:

: 3468-99-3
ethyl diphenylacetate

: 97634-33-8
4,4-diphenyl-5-methylhexan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaNH₂ / 1.) toluene, reflux, 15 min, 2.) toluene, reflux, 20 h

2: 90 percent / LiAlH₄ / diethyl ether / 5 h / Heating

3: CrO₃, 4.5 M H₂SO₄ / acetone / 0.17 h

4: 50 percent / benzoic acid / toluene / 80 h / Heating

5: H₂ / 10percent Pd/C / ethanol / 12 h / 2275.5 Torr

6: 90 percent / LiAlH₄ / diethyl ether / 5 h / Heating

With chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; hydrogen; sodium amide; benzoic acid; palladium on activated charcoal; In diethyl ether; ethanol; acetone; toluene;
DOI:10.1021/jm00149a014

Reference yield:

: 97634-30-5
2,2-diphenyl-3-methylbutyraldehyde

: 97634-33-8
4,4-diphenyl-5-methylhexan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / benzoic acid / toluene / 80 h / Heating

2: H₂ / 10percent Pd/C / ethanol / 12 h / 2275.5 Torr

3: 90 percent / LiAlH₄ / diethyl ether / 5 h / Heating

With lithium aluminium tetrahydride; hydrogen; benzoic acid; palladium on activated charcoal; In diethyl ether; ethanol; toluene;
DOI:10.1021/jm00149a014