C₂₅H₂₃FN₂O₇S

Base Information

Chemical Name:C₂₅H₂₃FN₂O₇S
CAS No.:1430475-95-8
Molecular Formula:C₂₅H₂₃FN₂O₇S
Molecular Weight:514.531
Hs Code.:

C<sub>25</sub>H<sub>23</sub>FN<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₅H₂₃FN₂O₇S

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Chemical Property of C₂₅H₂₃FN₂O₇S

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Technology Process of C₂₅H₂₃FN₂O₇S

There total 5 articles about C₂₅H₂₃FN₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430475-87-8
C₂₆H₂₅FN₂O₇S

: 1430475-95-8
C₂₅H₂₃FN₂O₇S

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2013.02.109

Reference yield:

: 1430475-80-1
C₂₆H₂₃FN₂O₇S

: 1430475-95-8
C₂₅H₂₃FN₂O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol

2: boron tribromide / dichloromethane / 2 h / 0 - 20 °C

With palladium 10% on activated carbon; hydrogen; boron tribromide; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2013.02.109

Reference yield:

: 1430475-71-0
ethyl 2-[N-(4-fluorophenyl)sulfamoyl]acetate

: 1430475-95-8
C₂₅H₂₃FN₂O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / water / 16 h / 20 °C

2: Lawessons reagent / neat (no solvent) / 2 h / 150 °C / Sealed tube

3: chloro-trimethyl-silane / N,N-dimethyl-formamide / 4 h / 135 °C / Sealed tube

4: palladium 10% on activated carbon; hydrogen / methanol

5: boron tribromide / dichloromethane / 2 h / 0 - 20 °C

With Lawessons reagent; chloro-trimethyl-silane; palladium 10% on activated carbon; hydrogen; boron tribromide; potassium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; 3: |Knoevenagel Condensation;
DOI:10.1016/j.bmcl.2013.02.109