tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

Base Information

Chemical Name:tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride
CAS No.:93660-99-2
Molecular Formula:C₃₃H₄₄N₆O₆S*ClH
Molecular Weight:689.276
Hs Code.:

Synonyms:tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

Chemical Property:

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Technology Process of tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

There total 12 articles about tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 62056-71-7
Nα-diphenylphosphinyltryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide

: 93660-99-2
tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 0 ℃; for 2.5h;

Reference yield:

: 7524-52-9,26988-71-6,5619-09-0,14907-27-8,41222-70-2,67557-19-1,109492-62-8
(S)-tryptophan methyl ester hydrochloride

: 93660-99-2
tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / N-methylmorpholine / CH₂Cl₂ / 0 °C

2: 90 percent / 2M sodium hydroxide / dioxane; methanol / 0.08 h / Ambient temperature

3: 65 percent / N-hydroxysuccinimide, DCC, N-methylmorpholine / dimethylformamide / 48 h / 0 °C

4: 78 percent / 1.5M HCl / methanol / 2.5 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 62056-82-0
Nα-dipnenylphosphinylmethionine

: 93660-99-2
tryptophanylmethionyl(β-t-butyl)aspartylphenylalanine amide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / N-hydroxysuccinimide, DCC / CH₂Cl₂ / 1.) 0 deg C, 2 h, 2.) room temperature, overnight

2: 70 percent / 4M HCl / H₂O; various solvent(s) / 5 h / Ambient temperature

3: 65 percent / N-hydroxysuccinimide, DCC, N-methylmorpholine / dimethylformamide / 48 h / 0 °C

4: 78 percent / 1.5M HCl / methanol / 2.5 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;