3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

Base Information

Chemical Name:3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole
CAS No.:634599-58-9
Molecular Formula:C₂₉H₃₄N₂O₄S
Molecular Weight:506.666
Hs Code.:

Synonyms:3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

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Chemical Property of 3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

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Technology Process of 3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

There total 1 articles about 3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2065-66-9
methyl-triphenylphosphonium iodide

: 3-[(1R,2R,3R,6S)-6-acetyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

: 634599-58-9
3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

Guidance literature:: With potassium tert-butylate; In toluene; at 55 - 60 ℃; for 8h;
DOI:10.1021/ja036191y

Reference yield:

: 634599-58-9
3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

: [(1R,2R,5R,6R)-6-(1H-Indol-3-yl)-5-isopropenyl-2-methyl-2-vinyl-cyclohexyl]-carbamic acid methyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 16h; Heating;
DOI:10.1021/ja036191y

Reference yield:

: 634599-58-9
3-[(1R,2R,3R,6S)-6-isopropenyl-3-methyl-2-(methoxycarbonyl)amino-3-vinylcyclohexyl]-1-tosyl-1H-indole

: (+)-hapalindole Q

Guidance literature:: Multi-step reaction with 2 steps

1: TBAF / tetrahydrofuran / 16 h / Heating

2: 12 mg / CH₂Cl₂ / 20 h / 0 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja036191y