N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

Base Information

• Chemical Name: N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin
• CAS No.: 90358-08-0
• Molecular Formula: C₅₅H₇₉N₈O₁₂PSi₃
• Molecular Weight: 1159.51

Synonyms:N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

Chemical Property of N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

Chemical Property:

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Safty Information:

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Technology Process of N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

There total 2 articles about N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

5'-O-<(p-Anisyl)diphenylmethyl>-N4-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-05-7) → N4-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-08-0)

Guidance literature:

With zinc dibromide; In methanol; nitromethane; for 0.0833333h;

Reference yield:

N4-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-<(4-methoxyphenyl)(diphenyl)methyl>tubercidin (87119-57-1) → N4-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-08-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sym-collidine / tetrahydrofuran / 0.5 h / -78 °C

2: 2.) I₂/H₂O / 1.) THF, 1 h, -78 deg C; 1 h, room temp, 2.) THF/sym-collidine, 15 min, room temp

3: 74 percent / ZnBr₂ / nitromethane; methanol / 0.08 h

With 2,4,6-trimethyl-pyridine; water; iodine; zinc dibromide; In tetrahydrofuran; methanol; nitromethane;

Reference yield: 97.0%

N4-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-08-0) + triethylamine (121-44-8) → N4-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(3'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz (90358-10-4)

Guidance literature:

With thiophenol; In 1,4-dioxane; for 0.75h; Ambient temperature;

upstream raw materials:

5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

N⁴-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-<(4-methoxyphenyl)(diphenyl)methyl>tubercidin

Downstream raw materials:

N⁴-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(3'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

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