2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

Base Information

Chemical Name:2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole
CAS No.:1251858-10-2
Molecular Formula:C₁₉H₁₇N₃O₂S
Molecular Weight:351.429
Hs Code.:

Synonyms:2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

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Chemical Property of 2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

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Technology Process of 2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

There total 2 articles about 2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 63617-18-5
5-(4-methoxybenzyl)-1,3,4-thiadiazol-2-amine

: 1251858-10-2
2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

Guidance literature:: 2-Bromo-4'-methoxyacetophenone; 5-(4-methoxybenzyl)-1,3,4-thiadiazol-2-amine; In ethanol; for 8h; Reflux;

With sodium carbonate; In water;

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 1251858-10-2
2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 8 h / 60 - 70 °C

2: potassium carbonate / ethanol / 12 h / Reflux

With sulfuric acid; potassium carbonate; In ethanol;
DOI:10.1002/cbdv.202000800

Reference yield: 85.0%

: 1251858-10-2
2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1251858-14-6
2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole-5-carbaldehyde

Guidance literature:: 2-(4-methoxybenzyl)-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole; N,N-dimethyl-formamide; With trichlorophosphate; at 0 - 60 ℃; for 4.5h;

With water; sodium carbonate; at 90 ℃; for 2h;