4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

Base Information

Chemical Name:4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester
CAS No.:1163791-20-5
Molecular Formula:C₃₀H₄₁N₅O₉
Molecular Weight:615.684
Hs Code.:

4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

Synonyms:4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

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Chemical Property of 4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

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Technology Process of 4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

There total 2 articles about 4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1164339-30-3
C₃₁H₄₃N₅O₉

: 1163791-20-5
4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

Guidance literature:: C₃₁H₄₃N₅O₉; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 0 ℃;

In tetrahydrofuran; methanol; water; pH=5; Acidic conditions;

Reference yield:

: 23426-63-3
2-bromo-2-methylpropionic acid methyl ester

: 1163790-65-5
4-{(S)-4-tert-butoxycarbonyl-2-[(5-hydroxy-1-phenyl-1H-pyrazole-3-carbonyl)-amino]-butyryl}-piperazine-1-carboxylic acid ethyl ester

: 1163791-20-5
4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

Guidance literature:: 2-bromo-2-methylpropionic acid methyl ester; 4-{(S)-4-tert-butoxycarbonyl-2-[(5-hydroxy-1-phenyl-1H-pyrazole-3-carbonyl)-amino]-butyryl}-piperazine-1-carboxylic acid ethyl ester; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

With lithium hydroxide; In tetrahydrofuran; methanol; water; at 0 ℃;

With hydrogenchloride; water; In tetrahydrofuran; methanol;

Reference yield:

: 60143-28-4
(S)-N-cyclopropylpyrrolidine-2-carboxamide hydrochloride

: 1163791-20-5
4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester

: C₃₈H₅₃N₇O₉

Guidance literature:: 4-((S)-4-tert-butoxycarbonyl-2-{[5-(1-carboxy-1-methyl-ethoxy)-1-phenyl-1H-pyrazole-3-carbonyl]-amino}-butyryl)-piperazine-1-carboxylic acid ethyl ester; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.333333h;

(S)-N-cyclopropylpyrrolidine-2-carboxamide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 6h;