2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

Base Information

Chemical Name:2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide
CAS No.:1345692-47-8
Molecular Formula:C₂₁H₁₆O₂S₄
Molecular Weight:428.621
Hs Code.:

Synonyms:2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

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Chemical Property of 2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

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Technology Process of 2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

There total 8 articles about 2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 107311-67-1
tributyl-(5-methylthiophen-2-yl)stannane

: 500772-42-9
2-bromo-3,5-dimethyl-6-phenyl-dithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

: 1345692-47-8
2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 80 ℃; for 1h; Microwave irradiation;
DOI:10.1021/ja2065522

Reference yield:

: 3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene

: 1345692-47-8
2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C / Darkness

2: N-Bromosuccinimide / dichloromethane; acetic acid / 0.5 h / 20 °C / Sonication

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 80 °C / Microwave irradiation

4: N-Bromosuccinimide / dichloromethane; acetic acid / 0.5 h / 20 °C / Sonication

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 80 °C / Microwave irradiation

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetic acid; toluene;
DOI:10.1021/ja2065522

Reference yield:

: 500772-34-9
2-bromo-3,5-dimethyl-dithieno[2,3-d:3',2'-b]thiophene-4,4-dioxide

: 1345692-47-8
2-phenyl-6-(2-methylthiophene)-3,5-dimethyldithieno[3,2-b:2',3'-d]thiophene-4,4-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 80 °C / Microwave irradiation

2: N-Bromosuccinimide / dichloromethane; acetic acid / 0.5 h / 20 °C / Sonication

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 1 h / 80 °C / Microwave irradiation

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; acetic acid; toluene;
DOI:10.1021/ja2065522