dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Base Information

Chemical Name:dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside
CAS No.:1115586-48-5
Molecular Formula:C₆₁H₇₇NO₁₃Si
Molecular Weight:1060.37
Hs Code.:

dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Synonyms:dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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Chemical Property of dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

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Technology Process of dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

There total 1 articles about dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 858525-75-4
2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: 1115586-48-5
dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside; In dichloromethane; at 20 ℃; for 2h; Molecular sieve; Inert atmosphere;

2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-glucopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 4h; Inert atmosphere;
DOI:10.1016/j.carres.2008.10.007

Reference yield: 77.0%

: 1115586-48-5
dimethyl t-hexylsilyl 2-O-benzoyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: 1115586-49-6
dimethyl t-hexylsilyl 3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1->4)-2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.carres.2008.10.007