(P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃

Base Information

• Chemical Name: (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃
• CAS No.: 700840-02-4
• Molecular Formula: CF₃O₃S*C₄₀H₄₁N₅P
• Molecular Weight: 771.843
• Mol file: 700840-02-4.mol

Synonyms:(P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃

Chemical Property of (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃

There total 1 articles about (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))⁽¹⁺⁾*SO₃CF₃^(1-) = (P(N((CH₃)3C₆H₂)CH₂)2)(CN(C₆H₅)C(C₆H₅)NN(C₆H₅))SO₃CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(1,3,4)-triphenyl-4,5-dihydro-1H-1,2,4-triazol-5-ylidene (166773-08-6) + [PN(2,4,6-Me3C6H2)CH2CH2N(2,4,6-Me3C6H2)](trifluoromethanesulfonate) → (P(N((CH3)3C6H2)CH2)2)(CN(C6H5)C(C6H5)NN(C6H5))(1+)*SO3CF3(1-) = (P(N((CH3)3C6H2)CH2)2)(CN(C6H5)C(C6H5)NN(C6H5))SO3CF3 (700840-02-4)

Guidance literature:

In dichloromethane;

DOI:10.1002/anie.200352326

Reference yield: 41.0%

tris(triphenylphosphine)platinum(0) (13517-35-6) + (P(N((CH3)3C6H2)CH2)2)(CN(C6H5)C(C6H5)NN(C6H5))(1+)*SO3CF3(1-) = (P(N((CH3)3C6H2)CH2)2)(CN(C6H5)C(C6H5)NN(C6H5))SO3CF3 (700840-02-4) → platinum(0)triphenylphosphine)(P(N-mesitylamino-CH2)2)(1,3,4-triphenyl-4,5-dihydro-1H-1,2,4-triazol-5-ylidene)triflate

Guidance literature:

In dichloromethane; C40H41N5PCF3SO3 added to soln. of Pt(PPh3)3 at -10°C, allowed to warm to roon temp. over 3 h, volatiles removed in vacuo; powder washed (toluene at 50°C);

DOI:10.1002/anie.200352326

upstream raw materials:

(1,3,4)-triphenyl-4,5-dihydro-1H-1,2,4-triazol-5-ylidene