Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

Base Information

Chemical Name:Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]
CAS No.:172295-97-5
Molecular Formula:C₅₀H₄₂P₃Rh
Molecular Weight:838.71
Hs Code.:

Rh(P(C<sub>6</sub>H<sub>5</sub>)3)[C<sub>6</sub>H<sub>3</sub>(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2]

Synonyms:Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

Suppliers and Price of Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

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Technology Process of Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

There total 10 articles about Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 172295-96-4
Rh(P(C₆H₅)3)[C₆H₃(CHCH₃)(CH₂P(C₆H₅)2)2]

: 172295-97-5
Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

Guidance literature:: With hydrogen; In toluene; byproducts: ethane; 20 psi H2, 120°C, 3 d;
DOI:10.1039/c39950001965

Reference yield: 95.0%

: 74219-49-1,40904-63-0
[RhCl(cyclooctene)]₂

: 603-35-0
triphenylphosphine

: 210363-34-1
1,3-Bis-[(diphenylphosphanyl)-methyl]-2-methoxy-benzene

: 172295-97-5
Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

Guidance literature:: With Et₃SiH; In 1,4-dioxane; byproducts: Et3SiCl, Et3SiOMe; (N2); stirring (30 min), addn. of (EtO)3SiH (pressure bottle, 130°C, ca. 30 min);
DOI:10.1021/ja9738889

Reference yield:

: 172295-98-6
[Rh(C₆H₃(CH₂P(C₆H₅)2)2)(P(C₆H₅)3)(H)(Cl)]

: 172295-97-5
Rh(P(C₆H₅)3)[C₆H₃(CH₂P(C₆H₅)2)2]

Guidance literature:: With NaH; In tetrahydrofuran; under N2; to a soln. of Rh complex in THF was added NaH, the mixt. was stirred for 24 h at 25°C; the soln. was evapd., the residue was dissolved in C6H6, ppt. was filtered, dried in vac.;
DOI:10.1021/ja000157r