(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

Base Information

Chemical Name:(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide
CAS No.:1332758-27-6
Molecular Formula:C₂₁H₃₂N₄O₆
Molecular Weight:436.508
Hs Code.:

Synonyms:(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

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Chemical Property of (2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

Chemical Property:

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Technology Process of (2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

There total 1 articles about (2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354939-11-9
(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanoic acid

: 1332758-27-6
(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

Guidance literature:: With 4-methyl-morpholine; ammonium chloride; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo202159q

Reference yield: 89.0%

: 1332757-98-8
(Z)-3-(benzyloxymethyl)-1-[2,3-di-O-(tert-butyldimethylsilyl)-4,5-dehydro-5-deoxy-5-iodo-β-D-ribopentofuranosyl]uracil

: 1332758-27-6
(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

: 1332758-13-0
C₅₀H₇₆N₆O₁₂Si₂

Guidance literature:: With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; at 70 ℃; for 7h; Inert atmosphere;
DOI:10.1021/jo202159q

Reference yield:

: 1332758-27-6
(2S,3S)-3-[(S)-2-(benzyloxycarbonylamino)-N-methylpropanamido]-2-(tert-butoxycarbonylamino)butanamide

: 1332758-21-0
C₃₈H₄₈N₆O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 7 h / 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With copper(l) iodide; tetrabutyl ammonium fluoride; caesium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran;
DOI:10.1021/jo202159q