3-Chloro-1-phenylpropan-1-ol

Base Information

Chemical Name:3-Chloro-1-phenylpropan-1-ol
CAS No.:18776-12-0
Molecular Formula:C9H11ClO
Molecular Weight:170.639
Hs Code.:
European Community (EC) Number:606-122-6
DSSTox Substance ID:DTXSID80341286
Nikkaji Number:J644.927A
Mol file:18776-12-0.mol

Synonyms:3-chloro-1-phenyl-propanol;3-chloro-1-phenylpropanol

Suppliers and Price of 3-Chloro-1-phenylpropan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
3-Chloro-1-phenyl-1-propanol
1g
$ 16.00

AK Scientific
3-Chloro-1-phenyl-1-propanol
25g
$ 75.00

American Custom Chemicals Corporation
3-CHLORO-1-PHENYL-PROPAN-1-OL 95.00%
50MG
$ 739.20

American Custom Chemicals Corporation
3-CHLORO-1-PHENYL-PROPAN-1-OL 95.00%
500MG
$ 1871.10

AstaTech
3-CHLORO-1-PHENYL-PROPANOL 97%
25 / G
$ 84.00

AstaTech
3-CHLORO-1-PHENYL-PROPANOL 97%
5 / G
$ 24.00

AstaTech
3-CHLORO-1-PHENYL-PROPANOL 97%
1 / G
$ 11.00

Chemcia Scientific
3-Chloro-1-phenyl-propan-1-ol ＞95%
100 G
$ 295.00

Chemenu
3-Chloro-1-phenyl-1-propanol 95+%
100g
$ 213.00

ChemScene
α-(2-Chloroethyl)benzenemethanol 99.60%
100g
$ 162.00

Total 98 raw suppliers

Chemical Property of 3-Chloro-1-phenylpropan-1-ol

Chemical Property:

Melting Point:31.0 to 36.0 °C
Refractive Index:1.54
Boiling Point:296.4 °C at 760 mmHg
PKA:13.92±0.20(Predicted)
Flash Point:132 °C
PSA：20.23000
Density:1.149 g/cm³
LogP:2.34890
Storage Temp.:0-10°C
Solubility.:Chloroform (Slightly), DMSO (Slightly), Ethyl Acetate (Slightly)
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:170.0498427
Heavy Atom Count:11
Complexity:99.7

Purity/Quality:

99.9% ^*data from raw suppliers

3-Chloro-1-phenyl-1-propanol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(CCCl)O
Uses An intermediate of racemic Atomoxetine.

Technology Process of 3-Chloro-1-phenylpropan-1-ol

There total 13 articles about 3-Chloro-1-phenylpropan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 936-59-4
3-chloropropiophenone

: 18776-12-0,125712-82-5
3-chloro-1-phenyl-propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1007/s11095-017-2271-7

Reference yield: 88.0%

: 1332887-24-7
3-chloro-1-phenylpropyl nitrate

: 18776-12-0,125712-82-5
3-chloro-1-phenyl-propan-1-ol

Guidance literature:: With diammonium sulfide; water; In ethanol; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2011.06.118

Reference yield: 65.0%

: 4850-49-1
1-phenyl-1,3-propanediol

: 18776-12-0,125712-82-5
3-chloro-1-phenyl-propan-1-ol

: 18775-64-9
(+/-)-3-chloro-3-phenylpropan-1-ol

Guidance literature:: 1-phenyl-1,3-propanediol; With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 ℃; for 0.25h; Inert atmosphere;

With chloro-trimethyl-silane; In toluene; at 20 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c3ob40853a