C₂₉H₄₁NO₄Si

Base Information

Chemical Name:C₂₉H₄₁NO₄Si
CAS No.:1265215-32-4
Molecular Formula:C₂₉H₄₁NO₄Si
Molecular Weight:495.734
Hs Code.:

C<sub>29</sub>H<sub>41</sub>NO<sub>4</sub>Si

Synonyms:C₂₉H₄₁NO₄Si

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Chemical Property of C₂₉H₄₁NO₄Si

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Technology Process of C₂₉H₄₁NO₄Si

There total 9 articles about C₂₉H₄₁NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1265214-91-2
C₂₉H₃₉NO₃Si

: 1265215-32-4
C₂₉H₄₁NO₄Si

Guidance literature:: C₂₉H₃₉NO₃Si; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 ℃; for 4h;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran;
DOI:10.1021/ol103024z

Reference yield:

: 1033282-40-4
diethyl 4-ethylideneheptanedioate

: 1265215-32-4
C₂₉H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.1: 1H-imidazole / dichloromethane / 2 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C

3.2: 0.5 h / -78 °C

4.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

5.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

6.1: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

With 1H-imidazole; dmap; lithium aluminium tetrahydride; oxalyl dichloride; potassium trimethylsilonate; palladium diacetate; potassium hexamethylsilazane; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Horner-Wadsworth-Emmons olefination / 5.1: Mizoroki-Heck cyclization;
DOI:10.1021/ol103024z

Reference yield:

: 1265214-87-6
C₂₅H₃₄O₂Si

: 1265215-32-4
C₂₉H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

3: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

5: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

With dmap; potassium trimethylsilonate; palladium diacetate; potassium hexamethylsilazane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 1: Horner-Wadsworth-Emmons olefination / 2: Mizoroki-Heck cyclization;
DOI:10.1021/ol103024z