ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

Base Information

Chemical Name:ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate
CAS No.:1379461-08-1
Molecular Formula:C₁₇H₁₃ClF₃NO₃
Molecular Weight:371.743
Hs Code.:

Synonyms:ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

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Chemical Property of ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

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Technology Process of ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

There total 1 articles about ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 1379461-07-0
2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)benzaldehyde

: 1379461-08-1
ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)benzaldehyde; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2012.03.036

Reference yield:

: 1379461-08-1
ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

: 2021-28-5
ethyl dihydrocinnamate

: 1379461-09-2
ethyl 3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)propanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 2h; under 760.051 Torr;
DOI:10.1016/j.bmc.2012.03.036

Reference yield:

: 1379461-08-1
ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate

: 1379461-26-3
3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2yl]oxy)-phenyl)propanoic acid

Guidance literature:: ethyl (2E)-3-(2-([3-chloro-5-(trifluoromethyl)pyridin-2-yl]oxy)phenyl)acrylate; With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 2h; under 760.051 Torr;

With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 50 ℃; for 0.5h;

With hydrogenchloride; In tetrahydrofuran; ethanol; water; at 20 ℃;
DOI:10.1016/j.bmc.2012.03.036