C₅₆H₆₄N₈O₁₁

Base Information

Chemical Name:C₅₆H₆₄N₈O₁₁
CAS No.:1321595-01-0
Molecular Formula:C₅₆H₆₄N₈O₁₁
Molecular Weight:1025.17
Hs Code.:

C<sub>56</sub>H<sub>64</sub>N<sub>8</sub>O<sub>11</sub>

Synonyms:C₅₆H₆₄N₈O₁₁

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Chemical Property of C₅₆H₆₄N₈O₁₁

Chemical Property:

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Technology Process of C₅₆H₆₄N₈O₁₁

There total 12 articles about C₅₆H₆₄N₈O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 888970-76-1
C₅₇H₆₆N₈O₁₁

: 1321595-01-0
C₅₆H₆₄N₈O₁₁

Guidance literature:: C₅₇H₆₆N₈O₁₁; With sodium hydroxide; In water; isopropyl alcohol; at 0 - 20 ℃; for 5h;

With citric acid; In methanol; water; at 0 ℃; pH=4;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 1048653-48-0
C₁₁H₁₅NO₂*ClH

: 1321595-01-0
C₅₆H₆₄N₈O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: HATU / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

1.2: 36 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 8 h / 20 °C / 760.05 Torr

3.1: HATU / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

3.2: 6 h / 20 °C / Inert atmosphere

3.3: 18 h / 20 °C / Inert atmosphere

4.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 20 °C / 760.05 Torr

5.1: HATU / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

5.2: 8 h / 20 °C / Inert atmosphere

5.3: 20 °C / Inert atmosphere

6.1: sodium hydroxide / water; isopropyl alcohol / 5 h / 0 - 20 °C

6.2: 0 °C / pH 4

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; HATU; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 888970-78-3
C₂₁H₂₄N₂O₅

: 1321595-01-0
C₅₆H₆₄N₈O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 8 h / 20 °C / 760.05 Torr

2.1: HATU / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

2.2: 6 h / 20 °C / Inert atmosphere

2.3: 18 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 20 °C / 760.05 Torr

4.1: HATU / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

4.2: 8 h / 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

5.1: sodium hydroxide / water; isopropyl alcohol / 5 h / 0 - 20 °C

5.2: 0 °C / pH 4

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; HATU; sodium hydroxide; In tetrahydrofuran; methanol; water; isopropyl alcohol;
DOI:10.1016/j.tet.2011.06.032