methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Base Information

Chemical Name:methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate
CAS No.:1446488-83-0
Molecular Formula:C₁₆H₂₀N₄O₅S
Molecular Weight:380.425
Hs Code.:

Synonyms:methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Suppliers and Price of methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

There total 7 articles about methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1267910-48-4
methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)thio]hept-2-en-1-yl carbonate

: 1446488-83-0
methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃; for 16h;
DOI:10.1021/jm400615g

Reference yield:

: 1446488-81-8
ethyl (2E)-7-[(1-Phenyl-1H-tetrazol-5-yl)thio]hept-2-enoate

: 1446488-83-0
methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / -78 °C

2: pyridine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / ethanol / 16 h / 0 - 20 °C

With pyridine; hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1021/jm400615g

Reference yield:

: 1446488-82-9
(2E)-7-[(1-phenyl-1H-tetrazol-5-yl)thio]hept-2-en-1-ol

: 1446488-83-0
methyl (2E)-7-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]hept-2-en-1-yl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / ethanol / 16 h / 0 - 20 °C

With pyridine; hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; dichloromethane;
DOI:10.1021/jm400615g