ethyl (1-13C)11-eicosenoate

Base Information

• Chemical Name: ethyl (1-13C)11-eicosenoate
• CAS No.: 153491-94-2
• Molecular Formula: C₂₂H₄₂O₂
• Molecular Weight: 339.563
• Mol file: 153491-94-2.mol

Synonyms:ethyl (1-13C)11-eicosenoate

Chemical Property of ethyl (1-13C)11-eicosenoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of ethyl (1-13C)11-eicosenoate

There total 1 articles about ethyl (1-13C)11-eicosenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Oleic aldehyde (2423-10-1) → ethyl (1-13C)11-eicosenoate (153491-94-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) diethyl ether, 2.) diethyl ether, 0 deg C, 30 min

2: (Ph₃PCuH)6, H₂O / benzene / 0.5 h

With hydrido(triphenylphosphine)copper(I) hexamer; water; sodium hydride; In benzene;

DOI:10.1002/jlcr.2580331003

Reference yield:

ethyl (1-13C)11-eicosenoate (153491-94-2) → (1-13C)11-eiconenoyl alcohol (153491-95-3)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Yield given; Heating;

DOI:10.1002/jlcr.2580331003

upstream raw materials:

Oleic aldehyde

Downstream raw materials:

(1-13C)11-eiconenoyl alcohol