Technology Process of C30H35N3O7
There total 9 articles about C30H35N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
tetrahydrofuran; methanol;
at 65 ℃;
for 12h;
DOI:10.1039/c2ob26262b
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sulfuric acid / 65 °C
2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 50 °C / Inert atmosphere
3: water; sodium hydroxide / tetrahydrofuran; methanol / 12 h / 65 °C
4: dichlorotriphenylphosphorane / chloroform / 80 °C / Inert atmosphere
5: palladium 10% on activated carbon; hydrogen / methanol / 6 h
6: water; sodium hydroxide / tetrahydrofuran; methanol / 12 h / 65 °C
With
sulfuric acid; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; sodium hydroxide; dichlorotriphenylphosphorane;
In
tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26262b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichlorotriphenylphosphorane / chloroform / 80 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / methanol / 6 h
3: water; sodium hydroxide / tetrahydrofuran; methanol / 12 h / 65 °C
With
palladium 10% on activated carbon; water; hydrogen; sodium hydroxide; dichlorotriphenylphosphorane;
In
tetrahydrofuran; methanol; chloroform;
DOI:10.1039/c2ob26262b
