C₃₆H₄₂O₁₁

Base Information

• Chemical Name: C₃₆H₄₂O₁₁
• CAS No.: 150843-11-1
• Molecular Formula: C₃₆H₄₂O₁₁
• Molecular Weight: 650.723
• Mol file: 150843-11-1.mol

Synonyms:C₃₆H₄₂O₁₁

Chemical Property of C₃₆H₄₂O₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₂O₁₁

There total 9 articles about C₃₆H₄₂O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C38H46O11 (150843-10-0) → C36H42O11 (150843-11-1)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)79162-3

Reference yield:

(4R,5S,6R)-5-Benzyloxy-4-hydroxy-2-methoxy-6-methyl-tetrahydro-pyran-2-carboxylic acid methyl ester (150843-05-3) → C36H42O11 (150843-11-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 percent / AgOTf, 4 Angstroem mol. sieves / CH₂Cl₂

2: 99 percent / aq. NaOH / tetrahydrofuran

With sodium hydroxide; 4 A molecular sieve; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;

DOI:10.1016/S0040-4039(00)79162-3

Reference yield:

(4R,5R,6R)-5-Benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-methoxy-6-methyl-tetrahydro-pyran-2-carboxylic acid methyl ester (150843-04-2) → C36H42O11 (150843-11-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 62 percent / camphor-10-sulfonic acid / methanol

2: 20 percent / AgOTf, 4 Angstroem mol. sieves / CH₂Cl₂

3: 99 percent / aq. NaOH / tetrahydrofuran

With sodium hydroxide; 4 A molecular sieve; camphor-10-sulfonic acid; silver trifluoromethanesulfonate; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1016/S0040-4039(00)79162-3

upstream raw materials:

C₃₈H₄₆O₁₁

(4R,5S,6R)-5-Benzyloxy-4-hydroxy-2-methoxy-6-methyl-tetrahydro-pyran-2-carboxylic acid methyl ester

(4R,5R,6R)-5-Benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-2-methoxy-6-methyl-tetrahydro-pyran-2-carboxylic acid methyl ester

((2R,3R,4R)-6-Benzenesulfonyl-3-benzyloxy-2-methyl-tetrahydro-pyran-4-yloxy)-tert-butyl-dimethyl-silane