1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

Base Information

Chemical Name:1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon
CAS No.:110315-50-9
Molecular Formula:C₁₉H₃₀O₅
Molecular Weight:338.444
Hs Code.:

Synonyms:1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

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Technology Process of 1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

There total 2 articles about 1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 110330-19-3
1-<(4,5-trans)-4,5-Dihydroxy-4-methyl-1-cyclohexen-1-yl>ethanon

: 110315-50-9
1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 24h; Ambient temperature;

Reference yield:

: 100938-99-6
1-(1-Methyl-7-oxabicyclo<4.1.0>hept-3-en-4-yl)ethanon

: 110315-50-9
1-<(4,5-trans)-4-Methyl-4,5-bis(tetrahydro-2-pyranyloxy)-1-cyclohexen-1-yl>ethanon

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 1percent H₂SO₄ / H₂O / 1 h / 70 °C

2: 54 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 24 h / Ambient temperature

With sulfuric acid; pyridinium p-toluenesulfonate; In dichloromethane; water;