Bis-(1-p-tolyl-ethyl)-amine

Base Information

Chemical Name:Bis-(1-p-tolyl-ethyl)-amine
CAS No.:52726-41-7
Molecular Formula:C₁₈H₂₃N
Molecular Weight:253.387
Hs Code.:

Synonyms:Bis-(1-p-tolyl-ethyl)-amine

Suppliers and Price of Bis-(1-p-tolyl-ethyl)-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis-(1-p-tolyl-ethyl)-amine

Chemical Property:

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Technology Process of Bis-(1-p-tolyl-ethyl)-amine

There total 4 articles about Bis-(1-p-tolyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27298-98-2
(S)-1-(4-methylphenyl)ethylamine

: 42070-98-4
1-(p-tolyl)ethylamine

: 52726-41-7
Bis-(1-p-tolyl-ethyl)-amine

Guidance literature:: With hydrogen; nickel; In toluene; at 70 ℃; for 24h; under 75.0075 Torr; Autoclave;
DOI:10.1002/adsc.200700336

Reference yield:

: 91854-79-4,113522-01-3
1-imino-1-(p-methylphenyl)ethane

: 52726-41-7
Bis-(1-p-tolyl-ethyl)-amine

Guidance literature:: With C₃₆H₁₇F₁₂NO₄S₂; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate; In tert-butyl methyl ether; at 23 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201608329

Reference yield:

: 104-85-8
para-methylbenzonitrile

: 52726-41-7
Bis-(1-p-tolyl-ethyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran / 2 h / -78 - -40 °C / Inert atmosphere

2: di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate; C₃₆H₁₇F₁₂NO₄S₂ / tert-butyl methyl ether / 23 °C / Molecular sieve; Inert atmosphere

With C₃₆H₁₇F₁₂NO₄S₂; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate; In tetrahydrofuran; diethyl ether; tert-butyl methyl ether;
DOI:10.1002/anie.201608329