(6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

Base Information

Chemical Name:(6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide
CAS No.:1252798-75-6
Molecular Formula:C₃₃H₃₄O₃P*I
Molecular Weight:636.509
Hs Code.:

Synonyms:(6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

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Chemical Property of (6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

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Technology Process of (6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

There total 1 articles about (6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1252798-74-5
(2R)-7-Iodo-1-[(4-methoxybenzyl)oxy]-4-heptyn-2-ol

: 603-35-0
triphenylphosphine

: 1252798-75-6
(6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

Guidance literature:: In acetonitrile; at 100 ℃; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201000565

Reference yield: 83.0%

: 1252798-75-6
(6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide

: 123-38-6
propionaldehyde

: 1252798-76-7
(2R,7Z)-1-[(4-methoxybenzyl)oxy]-7-decen-4-yn-2-ol

Guidance literature:: (6R)-6-hydroxy-7-[(4-methoxybenzyl)oxy]-3-heptynyl(triphenyl)phosphonium Iodide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h; Inert atmosphere;

propionaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejoc.201000565