Z-Pro-OCamp

Base Information

• Chemical Name: Z-Pro-OCamp
• CAS No.: 98807-05-7
• Molecular Formula: C₂₃H₂₈N₂O₆
• Molecular Weight: 428.485

Synonyms:Z-Pro-OCamp

Chemical Property of Z-Pro-OCamp

Chemical Property:

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Technology Process of Z-Pro-OCamp

There total 1 articles about Z-Pro-OCamp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.6%

N-hydroxycamphorimide (98919-82-5) + N-Benzyloxycarbonyl-L-proline (1148-11-4) → Z-Pro-OCamp (98807-05-7)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;

Reference yield:

DL-leucine ethyl ester hydrochloride (2743-40-0,23420-04-4,73913-65-2) + Z-Pro-OCamp (98807-05-7) → N-(N-benzyloxycarbonyl-L-prolyl)-L-leucine ethyl ester (54769-24-3) + Z-L-Pro-D-Leu-OEt (98807-12-6)

Guidance literature:

With sodium acetate; In acetonitrile; for 168h; Yield given; Ambient temperature;

Reference yield:

ethyl 2-amino-3-phenylpropanoate hydrochloride (3182-93-2) + Z-Pro-OCamp (98807-05-7) → Z-L-Pro-D-Phe-OEt (98807-11-5) + Z-L-Pro-L-Phe-OEt (18532-06-4)

Guidance literature:

With sodium acetate; toluene-4-sulfonic acid; acetic acid; In acetonitrile; for 504h; Yield given; Ambient temperature;

upstream raw materials:

N-hydroxycamphorimide

N-Benzyloxycarbonyl-L-proline

Downstream raw materials:

Z-L-Pro-L-Ala-OEt

Z-L-Pro-D-Ala-OEt

Z-L-Pro-D-Phe-OEt

Z-L-Pro-L-Phe-OEt

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