(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose

Base Information

• Chemical Name: (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose
• CAS No.: 1204403-22-4
• Molecular Formula: C₅₀H₄₆O₁₆
• Molecular Weight: 902.906

Synonyms:(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose

Chemical Property of (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose

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Technology Process of (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose

There total 2 articles about (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C57H52O15S (1193366-67-4) → (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose (1204403-22-4)

Guidance literature:

With N-Bromosuccinimide; water; In acetone; at 20 ℃; for 1h;

DOI:10.1002/ejoc.200900778

Reference yield:

allyl (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside → (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose (1204403-22-4) + (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranose (1597422-08-6)

Guidance literature:

allyl (2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside; With sodium acetate; acetic acid; palladium dichloride; In water; at 70 ℃; for 3h;

With camphor-10-sulfonic acid; 2,2-dimethoxy-propane; In acetone; for 0.5h;

DOI:10.1007/s11172-014-0462-5

Reference yield: 98.0%

(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranose (1204403-22-4) + trichloroacetonitrile (545-06-2) → (2,6-Di-O-benzoyl-3,4-di-O-isopropylidene-ν-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl trichloroacetimidate

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/ejoc.200900778

upstream raw materials:

C₅₇H₅₂O₁₅S

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