C₂₀H₁₇IO₂

Base Information

• Chemical Name: C₂₀H₁₇IO₂
• CAS No.: 1353441-26-5
• Molecular Formula: C₂₀H₁₇IO₂
• Molecular Weight: 416.258
• Mol file: 1353441-26-5.mol

Synonyms:C₂₀H₁₇IO₂

Chemical Property of C₂₀H₁₇IO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₀H₁₇IO₂

There total 2 articles about C₂₀H₁₇IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C20H18O2 → C20H17IO2 (1353441-26-5)

Guidance literature:

With iodine; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 8h;

DOI:10.1055/s-0030-1260196

Reference yield:

4-tolyl iodide (624-31-7) + C13H12O2 (59155-68-9) → C20H17IO2 (1353441-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 5 h / 20 °C

2: iodine; sodium hydrogencarbonate / acetonitrile / 8 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; sodium hydrogencarbonate; triethylamine; In N,N-dimethyl-formamide; acetonitrile; 1: Sonogashira coupling reaction;

DOI:10.1055/s-0030-1260196

upstream raw materials:

4-tolyl iodide

C₁₃H₁₂O₂