Technology Process of C13H17BrO4
There total 1 articles about C13H17BrO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,4-dibromo-2,5-bis(methoxymethoxy)benzene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.333333h;
Inert atmosphere;
With
copper(l) iodide;
In
tetrahydrofuran; hexane;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
allyl bromide;
In
tetrahydrofuran; hexane;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1021/ja106813s
- Guidance literature:
-
C13H17BrO4;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.25h;
Inert atmosphere;
1-bromo-3,7,11-trimethyldodeca-2(Z),6(E),10-triene;
In
tetrahydrofuran; hexane;
at -40 - 5 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja106813s
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.25 h / -78 °C / Inert atmosphere
1.2: 2 h / -40 - 5 °C / Inert atmosphere
2.1: bromodiethylsulfonium bromopentachloroantimonate / nitromethane / 0.08 h / -25 °C / Inert atmosphere
2.2: 1 h / -25 °C
3.1: osmium(VIII) oxide; sodium periodate; pyridine; water / tert-butyl alcohol; tetrahydrofuran / 2 h / 0 - 25 °C
4.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogen phosphate monohydrate / water / 0.33 h / 0 °C
5.1: boron trichloride / dichloromethane / 1 h / -78 °C
With
pyridine; sodium chlorite; sodium periodate; osmium(VIII) oxide; n-butyllithium; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; boron trichloride;
bromodiethylsulfonium bromopentachloroantimonate;
In
tetrahydrofuran; hexanes; nitromethane; dichloromethane; water; tert-butyl alcohol;
