9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene

Base Information

• Chemical Name: 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene
• CAS No.: 1112955-34-6
• Molecular Formula: C₃₃H₃₁NO
• Molecular Weight: 457.615
• Mol file: 1112955-34-6.mol

Synonyms:9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene

Chemical Property of 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene

There total 2 articles about 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C32H28NO (1112955-33-5) + dimethyl sulfoxide (67-68-5,8070-53-9) → 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene (1112955-34-6)

Guidance literature:

With FeO₃S^(2-)*Fe⁽²⁺⁾*7H₂O; dihydrogen peroxide; In water;

DOI:10.1039/c3cc46146g

Reference yield: 88.0%

4,4,5,5-tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane (460347-59-5) + 5-iodo-2-methoxy-1,1,3,3-tetramethylisoindoline (955959-04-3) → 9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene (1112955-34-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 80 ℃; for 72h; Inert atmosphere;

DOI:10.1002/ejoc.200800597

Reference yield: 75.0%

9-(2-methoxy-1,1,3,3-tetramethylisoindolin-5-yl)-10-phenylanthracene (1112955-34-6) → C32H28NO (1112955-33-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h; Time;

DOI:10.1039/c3cc46146g

upstream raw materials:

4,4,5,5-tetramethyl-2-(10-phenylanthracen-9-yl)-1,3,2-dioxaborolane

5-iodo-2-methoxy-1,1,3,3-tetramethylisoindoline

C₃₂H₂₈NO

dimethyl sulfoxide

Downstream raw materials:

C₃₂H₂₈NO