Technology Process of 2-diazo-5,6-di(m-tolyl)acenaphthenone
There total 5 articles about 2-diazo-5,6-di(m-tolyl)acenaphthenone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
dichloromethane;
DOI:10.1021/jo040175h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Mg / diethyl ether / 0.5 h / Heating
1.2: 44 percent / nickel acetylacetonate / diethyl ether; benzene / 20 °C
2.1: 28 percent / AlCl3 / CS2 / 3 h
3.1: 100 percent / methanol / 5 h / Heating
4.1: 84 percent / aq. NaOH / CH2Cl2
With
sodium hydroxide; aluminium trichloride; magnesium;
In
methanol; carbon disulfide; diethyl ether; dichloromethane;
DOI:10.1021/jo040175h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Mg / diethyl ether / 0.5 h / Heating
1.2: 44 percent / nickel acetylacetonate / diethyl ether; benzene / 20 °C
2.1: 28 percent / AlCl3 / CS2 / 3 h
3.1: 100 percent / methanol / 5 h / Heating
4.1: 84 percent / aq. NaOH / CH2Cl2
With
sodium hydroxide; aluminium trichloride; magnesium;
In
methanol; carbon disulfide; diethyl ether; dichloromethane;
DOI:10.1021/jo040175h
