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C24H33N5O8

Base Information
  • Chemical Name:C24H33N5O8
  • CAS No.:1469300-23-9
  • Molecular Formula:C24H33N5O8
  • Molecular Weight:519.555
  • Hs Code.:
C<sub>24</sub>H<sub>33</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:C24H33N5O8

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Chemical Property of C24H33N5O8
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Technology Process of C24H33N5O8

There total 11 articles about C24H33N5O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201304239
Guidance literature:
Multi-step reaction with 6 steps
1.1: boron trifluoride diethyl etherate / acetonitrile / 0.17 h / 0 °C / Inert atmosphere
2.1: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr
4.1: lithium hydroxide monohydrate; water / d(4)-methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
5.2: 12 h / 20 °C / Inert atmosphere
6.1: lithium hydroxide monohydrate; water / methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With lithium hydroxide monohydrate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; d(4)-methanol; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201304239
Guidance literature:
Multi-step reaction with 6 steps
1.1: potassium tert-butylate / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere
2.1: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr
4.1: lithium hydroxide monohydrate; water / d(4)-methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
5.2: 12 h / 20 °C / Inert atmosphere
6.1: lithium hydroxide monohydrate; water / methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With lithium hydroxide monohydrate; palladium 10% on activated carbon; potassium tert-butylate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; d(4)-methanol; ethyl acetate;
DOI:10.1002/anie.201304239
upstream raw materials:

C12H21NO6

C12H20N4O5

C19H27NO6

C25H35N5O8

Downstream raw materials:

C44H58N10O13

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