Technology Process of diethyl 2-malonate
There total 4 articles about diethyl 2-malonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 2h;
under 2068.6 Torr;
DOI:10.1002/jhet.5570300544
- Guidance literature:
-
With
hydrogen; acetic acid;
palladium on activated charcoal;
for 1h;
under 2068.6 Torr;
DOI:10.1002/jhet.5570300544
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 1,1'-carbonyldiimidazole, 2.) triethylamine / 1.) THF, reflux. 4 h, 2.) THF, methylene chloride, RT, 1 h
2: 82 percent / H2 / 10percent Pd/C / methanol / 2 h / 2068.6 Torr
With
hydrogen; triethylamine; 1,1'-carbonyldiimidazole;
palladium on activated charcoal;
In
methanol;
DOI:10.1002/jhet.5570300544
