(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

Base Information

Chemical Name:(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine
CAS No.:408347-72-8
Molecular Formula:C₁₆H₃₀N₃PSi
Molecular Weight:323.494
Hs Code.:

(1,3-di-<i>tert</i>-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

Synonyms:(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

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Chemical Property of (1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

Chemical Property:

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Technology Process of (1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

There total 1 articles about (1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20732-26-7,82959-02-2
lithium anilide

: 77382-31-1
1,3-Di-tert-butyl-2-chlor-4,4-dimethyl-1,3-diaza-2-phospha-4-silacyclobutan

: 408347-72-8
(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

Guidance literature:: DOI:10.1080/10426500490427213

Reference yield: 64.9%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 408347-72-8
(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

: (1,3-di-tert-butyl-2-diphenylphosphanyl-4,4-dimethyl-2λ⁵-[1,3,2,4]diazaphosphasiletidin-2-ylidene)-phenyl-amine

Guidance literature:: With n-butyllithium; In hexane; at 20 ℃;
DOI:10.1002/anie.200462588

Reference yield:

: 408347-72-8
(1,3-di-tert-butyl-4,4-dimethyl-[1,3,2,4]diazaphosphasiletidin-2-yl)-phenyl-amine

: [1,3-di-tert-butyl-2-(diphenyl-phosphinothioyl)-4,4-dimethyl-2λ⁵-[1,3,2,4]diazaphosphasiletidin-2-ylidene]-phenyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 64.9 percent / n-BuLi / hexane / 20 °C

2: 81.2 percent / S₈ / tetrahydrofuran / 3 h / Heating

With sulfur; n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1002/anie.200462588