8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

Base Information

Chemical Name:8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline
CAS No.:865981-82-4
Molecular Formula:C₂₀H₁₉N₃O₃
Molecular Weight:349.389
Hs Code.:

Synonyms:8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

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Chemical Property of 8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

Chemical Property:

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Technology Process of 8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

There total 8 articles about 8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 620949-49-7
8-methoxy-6-methyl-5-nitro-4-phenylquinoline

: 865981-82-4
8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

Guidance literature:: With triethylamine; at 145 ℃; for 48h;
DOI:10.3987/COM-05-10442

Reference yield: 91.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 620949-49-7
8-methoxy-6-methyl-5-nitro-4-phenylquinoline

: 865981-82-4
8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

Guidance literature:: at 170 ℃; for 96h;
DOI:10.3987/COM-03-9827

Reference yield:

: 620949-48-6
4-bromo-8-methoxy-6-methyl-5-nitroquinoline

: 865981-82-4
8-methoxy-6-[β-trans-(N,N-dimethylamino)ethenyl]-5-nitro-4-phenylquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. K₂CO₃ / tetrakis(triphenylphosphine)palladium catalyst / toluene; ethanol / 3 h / 95 °C

2: 91 percent / triethylamine / 48 h / 145 °C

With potassium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene;
DOI:10.3987/COM-05-10442