(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

Base Information

Chemical Name:(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol
CAS No.:244203-41-6
Molecular Formula:C₁₇H₂₄O₄
Molecular Weight:292.375
Hs Code.:

Synonyms:(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

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Chemical Property of (1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

Chemical Property:

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Technology Process of (1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

There total 6 articles about (1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,3-O-isopropylidene-L-erythrose

: 244203-41-6
(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: 3.13 g / tetrahydrofuran; hexane / 2.5 h / -55 - 20 °C

2: 99 percent / K₂CO₃; H₂ / Pd/C / ethyl acetate / 9 h / 20 °C

3: 100 percent / pyridine / CH₂Cl₂ / 0.33 h / -15 °C

With pyridine; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate;
DOI:10.1021/ol990102y

Reference yield:

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 244203-41-6
(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaBH₄ / H₂O / 1 h / 20 °C

1.2: 9.2 g / NaIO₄ / H₂O / 2 h / 0 °C

2.1: 3.13 g / tetrahydrofuran; hexane / 2.5 h / -55 - 20 °C

3.1: 99 percent / K₂CO₃; H₂ / Pd/C / ethyl acetate / 9 h / 20 °C

4.1: 100 percent / pyridine / CH₂Cl₂ / 0.33 h / -15 °C

With pyridine; sodium tetrahydroborate; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; water; ethyl acetate;
DOI:10.1021/ol990102y

Reference yield:

: 139727-13-2
[(4S,5R)-2,2-Dimethyl-5-(2-methyl-propenyl)-[1,3]dioxolan-4-yl]-methanol

: 244203-41-6
(1'S,5'R)-3-{[3',3'-dimethyl-5'-(2''-methylpropyl)(2',4'-dioxolanyl)]methyl}-2-formylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / K₂CO₃; H₂ / Pd/C / ethyl acetate / 9 h / 20 °C

2: 100 percent / pyridine / CH₂Cl₂ / 0.33 h / -15 °C

With pyridine; hydrogen; potassium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ol990102y