(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Base Information

Chemical Name:(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate
CAS No.:1359852-06-4
Molecular Formula:C₂₁H₃₁NO₅
Molecular Weight:377.481
Hs Code.:

Synonyms:(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Suppliers and Price of (S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

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Chemical Property of (S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Chemical Property:

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Technology Process of (S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

There total 1 articles about (S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: 2462-34-2
L-valine benzyl ester hydrochloride

: 1359852-06-4
(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;

Reference yield:

: 1359852-06-4
(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

: 1359852-76-8
methyl 8-((2S)-1-(1-(4-(benzyloxy)phenyl)-3-hydroxypropan-2-ylamino)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: potassium carbonate / acetone / 20 °C / Inert atmosphere

With hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1359852-06-4
(S)-methyl 8-(1-(benzyloxy)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

: 1359852-70-2
methyl 8-((2S)-1-(1-(4-(benzyloxy)-phenyl)-3-oxopropan-2-ylamino)-3-methyl-1-oxobutan-2-ylamino)-8-oxooctanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 4 h / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: potassium carbonate / acetone / 20 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere

With hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; palladium 10% on activated carbon; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;