C₁₇H₂₁FN₄O₇S

Base Information

Chemical Name:C₁₇H₂₁FN₄O₇S
CAS No.:1402742-21-5
Molecular Formula:C₁₇H₂₁FN₄O₇S
Molecular Weight:444.441
Hs Code.:

C<sub>17</sub>H<sub>21</sub>FN<sub>4</sub>O<sub>7</sub>S

Synonyms:C₁₇H₂₁FN₄O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₁FN₄O₇S

Chemical Property:

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Technology Process of C₁₇H₂₁FN₄O₇S

There total 21 articles about C₁₇H₂₁FN₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₁FN₄O₇S

: 1402742-22-6
C₁₇H₂₁FN₄O₇S

: 1402742-21-5
C₁₇H₂₁FN₄O₇S

Guidance literature:: With carbon dioxide; ammonia; In methanol; water; at 38 ℃; Purification / work up; Resolution of racemate;

Reference yield:

: 1402742-06-6
C₂₈H₃₂FNO₆S

: 1402742-22-6
C₁₇H₂₁FN₄O₇S

: 1402742-21-5
C₁₇H₂₁FN₄O₇S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - -30 °C

1.2: -78 - 25 °C

2.1: hydrogen / palladium hydrogenation catalyst / ethanol

3.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 60 °C

4.2: 25 °C / pH 3

5.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C

5.2: 1.5 h / 80 °C

6.1: trifluoroacetic acid / 1,3-Dimethoxybenzene; chloroform / 18 h

7.1: 4 h / Reflux

7.2: 12 h / 25 °C

8.1: nitric acid; sulfuric acid / 1 h / -10 °C

8.2: 12 h / 30 °C

9.1: carbon dioxide; ammonia / water; methanol / 38 °C / Resolution of racemate

With carbon dioxide; sulfuric acid; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; ammonia; water; hydrogen; nitric acid; sodium hexamethyldisilazane; triethylamine; trifluoroacetic acid; lithium hydroxide; palladium hydrogenation catalyst; In tetrahydrofuran; methanol; ethanol; chloroform; water; toluene; 1,3-Dimethoxybenzene;

Reference yield:

: 1402742-07-7
C₂₉H₃₄FNO₇S

: 1402742-22-6
C₁₇H₂₁FN₄O₇S

: 1402742-21-5
C₁₇H₂₁FN₄O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogen / palladium hydrogenation catalyst / ethanol

2.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C

3.1: water; lithium hydroxide / tetrahydrofuran / 60 °C

3.2: 25 °C / pH 3

4.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C

4.2: 1.5 h / 80 °C

5.1: trifluoroacetic acid / 1,3-Dimethoxybenzene; chloroform / 18 h

6.1: 4 h / Reflux

6.2: 12 h / 25 °C

7.1: nitric acid; sulfuric acid / 1 h / -10 °C

7.2: 12 h / 30 °C

8.1: carbon dioxide; ammonia / water; methanol / 38 °C / Resolution of racemate

With carbon dioxide; sulfuric acid; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; ammonia; water; hydrogen; nitric acid; triethylamine; trifluoroacetic acid; lithium hydroxide; palladium hydrogenation catalyst; In tetrahydrofuran; methanol; ethanol; chloroform; water; toluene; 1,3-Dimethoxybenzene;