N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

Base Information

Chemical Name:N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine
CAS No.:259748-15-7
Molecular Formula:C₁₉H₂₀Br₂N₂O₂
Molecular Weight:468.188
Hs Code.:

Synonyms:N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

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Technology Process of N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

There total 1 articles about N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

: 1761-61-1
5-bromosalicyclaldehyde

: 259748-15-7
N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

Guidance literature:: In ethanol; for 1h; Reflux;
DOI:10.1016/j.poly.2017.05.049

Reference yield: 81.0%

: sodium azide

: manganese(II) chloride dihydrate

: 259748-15-7
N,N'-bis(5-bromo-2-hydroxybenzylidene)-2,2-dimethylpropane-1,3-diamine

: 1323980-17-1
[manganese(III)(N,N'-bis(5-bromosalicylidene)-2,2-dimethyl-1,3-propanediamine(-2H))(μ1,3-N3)]n

Guidance literature:: In methanol; water; acetone; H2BrSal2MePn dissolved in methanol-acetone with stirring, methanol soln.of MnCl2*2H2O added, stirred for 2 h at room temp., aq. soln. of sodium azide slowly added dropwise, soln. stirred for 20 min at room temp.; filtration, evapn., drying in vacuo, elem. anal.;
DOI:10.1134/S1070328411070074