2-methoxy-2'-methyl-N-propyldiphenylamine

Base Information

Chemical Name:2-methoxy-2'-methyl-N-propyldiphenylamine
CAS No.:78966-63-9
Molecular Formula:C₁₇H₂₁NO
Molecular Weight:255.36
Hs Code.:

Synonyms:2-methoxy-2'-methyl-N-propyldiphenylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methoxy-2'-methyl-N-propyldiphenylamine

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Technology Process of 2-methoxy-2'-methyl-N-propyldiphenylamine

There total 6 articles about 2-methoxy-2'-methyl-N-propyldiphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 78943-70-1
N-propyl-2-hydroxy-2'-methyldiphenylamine

: 77-78-1
dimethyl sulfate

: 78966-63-9
2-methoxy-2'-methyl-N-propyldiphenylamine

Guidance literature:: With sodium hydroxide; In methanol; acetone; for 0.333333h; Ambient temperature;
DOI:10.1248/cpb.29.1221

Reference yield: 53.7%

: 78943-67-6
N-(2-methoxyphenyl)-N-(2-methylphenyl)amine

: 106-94-5
propyl bromide

: 78966-63-9
2-methoxy-2'-methyl-N-propyldiphenylamine

Guidance literature:: With sodium amide; In toluene; for 2h; Heating;
DOI:10.1248/cpb.29.1221

Reference yield:

: 95-46-5
2-methylphenyl bromide

: 78966-63-9
2-methoxy-2'-methyl-N-propyldiphenylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 19 percent / anhydrous K₂CO₃, Cu, I₂ / 28 h / 200 °C

2: 44.3 percent / LiAlH₄ / tetrahydrofuran / 0.33 h / Ambient temperature

3: 53.7 percent / sodium amide / toluene / 2 h / Heating

With lithium aluminium tetrahydride; iodine; copper; potassium carbonate; sodium amide; In tetrahydrofuran; toluene;
DOI:10.1248/cpb.29.1221