C₅₃H₆₃FO₂₂

Base Information

Chemical Name:C₅₃H₆₃FO₂₂
CAS No.:97974-27-1
Molecular Formula:C₅₃H₆₃FO₂₂
Molecular Weight:1071.07
Hs Code.:

C<sub>53</sub>H<sub>63</sub>FO<sub>22</sub>

Synonyms:C₅₃H₆₃FO₂₂

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Chemical Property of C₅₃H₆₃FO₂₂

Chemical Property:

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Technology Process of C₅₃H₆₃FO₂₂

There total 10 articles about C₅₃H₆₃FO₂₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 97974-26-0
C₅₉H₆₈O₂₂S

: 97974-27-1
C₅₃H₆₃FO₂₂

Guidance literature:: With N-Bromosuccinimide; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at -15 ℃; for 1h;
DOI:10.1021/ja00305a056

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 97974-27-1
C₅₃H₆₃FO₂₂

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / CSA / benzene / 25 °C

2: 90 percent / NaH / tetrahydrofuran / Heating

3: 1.) NaCNBH₃, 4 A mol. sieves; 2.) HCl(g) / 1.) THF, 25 deg C; 2.) Et₂O

4: 75 percent / SnCl₂, AgClO₄, 4 A mol. sieves / CH₂Cl₂ / 18 h / -15 °C

5: 85 percent / NBS, DAST / CH₂Cl₂ / 1 h / -15 °C

With hydrogenchloride; N-Bromosuccinimide; 4 A molecular sieve; camphor-10-sulfonic acid; silver perchlorate; sodium hydride; sodium cyanoborohydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja00305a056

Reference yield:

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 97974-27-1
C₅₃H₆₃FO₂₂

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / CSA / benzene / 25 °C

2: 90 percent / NaH / tetrahydrofuran / Heating

3: 1.) NaCNBH₃, 4 A mol. sieves; 2.) HCl(g) / 1.) THF, 25 deg C; 2.) Et₂O

4: 75 percent / SnCl₂, AgClO₄, 4 A mol. sieves / CH₂Cl₂ / 18 h / -15 °C

5: 85 percent / NBS, DAST / CH₂Cl₂ / 1 h / -15 °C

With hydrogenchloride; N-Bromosuccinimide; 4 A molecular sieve; camphor-10-sulfonic acid; silver perchlorate; sodium hydride; sodium cyanoborohydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/ja00305a056