2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

Base Information Edit

Chemical Name:2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal
CAS No.:129929-20-0
Molecular Formula:C₃₆H₅₄O₅S₂
Molecular Weight:630.954
Hs Code.:
Mol file:129929-20-0.mol

2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

Synonyms:2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

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Chemical Property of 2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal Edit

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Technology Process of 2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

There total 5 articles about 2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100699-20-5
2,4-dideoxy-5,6-O-isopropylidene-2,4-di-C-methyl-D-glucose trimethylene dithioacetal

: 129929-20-0
2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium hydride / 1) N,N-dimethylformamide, 4h, 20 deg C, 2) 15h

2: 87 percent / aq. hydrochloric acid / tetrahydrofuran / 80 h / 20 °C

3: 86 percent / potassium acetate, lead tetra-acetate / acetonitrile / 0.05 h / -25 °C

With lead(IV) acetate; hydrogenchloride; potassium acetate; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1016/0008-6215(90)84192-W

Reference yield:

: 129908-72-1
2,4-dideoxy-3-O-(p-methoxybenzyl)-2,4-di-C-methyl-D-glucose trimethylene dithioacetal

: 129929-20-0
2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / potassium acetate, lead tetra-acetate / acetonitrile / 0.05 h / -25 °C

With lead(IV) acetate; potassium acetate; In acetonitrile;
DOI:10.1016/0008-6215(90)84192-W

Reference yield:

: 129908-71-0
2,4-dideoxy-5,6-O-isopropylidene-3-O-(p-methoxybenzyl)-2,4-di-C-methyl-D-glucose trimethylene dithioacetal

: 129929-20-0
2,6-di-tert-butyl-4-methylphenyl 2,4,6-trideoxy-3-O-(p-methoxybenzyl)-2,4,6-tri-C-methyl-L-glycero-L-ido-hepturonate trimethylene dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / aq. hydrochloric acid / tetrahydrofuran / 80 h / 20 °C

2: 86 percent / potassium acetate, lead tetra-acetate / acetonitrile / 0.05 h / -25 °C

With lead(IV) acetate; hydrogenchloride; potassium acetate; In tetrahydrofuran; acetonitrile;
DOI:10.1016/0008-6215(90)84192-W