Technology Process of C26H26O5
There total 4 articles about C26H26O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine; dmap / 16 h / 20 °C
2: hydrogenchloride / dichloromethane / 17 h / 0 - 15 °C / Sealed tube
3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Heating
4: ammonia / methanol / 16 h / 20 °C / Sealed tube
5: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C
With
pyridine; hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride;
In
methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol401730d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / dichloromethane / 17 h / 0 - 15 °C / Sealed tube
2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Heating
3: ammonia / methanol / 16 h / 20 °C / Sealed tube
4: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C
With
hydrogenchloride; 2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride;
In
methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol401730d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Heating
2: ammonia / methanol / 16 h / 20 °C / Sealed tube
3: camphorsulphonic acid / N,N-dimethyl-formamide / 4 h / 55 °C
With
2,2'-azobis(isobutyronitrile); ammonia; tri-n-butyl-tin hydride;
In
methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol401730d
