o-diphenylphosphonylbenzoic acid methyl ester

Base Information

Chemical Name:o-diphenylphosphonylbenzoic acid methyl ester
CAS No.:79317-63-8
Molecular Formula:C₂₀H₁₇O₃P
Molecular Weight:336.327
Hs Code.:

Synonyms:o-diphenylphosphonylbenzoic acid methyl ester

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Chemical Property of o-diphenylphosphonylbenzoic acid methyl ester

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Technology Process of o-diphenylphosphonylbenzoic acid methyl ester

There total 13 articles about o-diphenylphosphonylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: methyl 2-((diphenylphosphoryl)carbonyl)benzoate

: 79317-63-8
o-diphenylphosphonylbenzoic acid methyl ester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; In 5,5-dimethyl-1,3-cyclohexadiene; at 130 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2020.131912

Reference yield: 70.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 2572-40-9
(o-carboxyphenyl)diphenylphosphine oxide

: 79317-63-8
o-diphenylphosphonylbenzoic acid methyl ester

Guidance literature:: In diethyl ether; benzene;
DOI:10.1007/BF01417991

Reference yield: 55.0%

: 610-94-6
2-bromobenzoic acid methyl ester

: 4559-70-0
Diphenylphosphine oxide

: 79317-63-8
o-diphenylphosphonylbenzoic acid methyl ester

Guidance literature:: With thio-xanthene-9-one; N-isopropyl-N-tert-butylamine; 4,4'-di-tert-butyl-2,2'-bipyridine; nickel dibromide; In acetonitrile; for 24h; Irradiation; Inert atmosphere;
DOI:10.1021/acs.orglett.0c03892