2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Base Information

Chemical Name:2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline
CAS No.:868847-11-4
Molecular Formula:C₂₄H₂₄N₂O₂S
Molecular Weight:404.533
Hs Code.:

Synonyms:2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

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Technology Process of 2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

There total 6 articles about 2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6502-82-5
N_b-formyltryptamine

: 868847-11-4
2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃ / CH₂Cl₂ / 16 h / 0 °C

2: 78 percent / Cs₂CO₃; K₂CO₃ / dimethylformamide / 16 h / 20 °C

3: 76 percent / tetrahydrofuran / 20 °C

4: 83 percent / NaH / tetrahydrofuran / 0 - 20 °C

With sodium hydride; potassium carbonate; caesium carbonate; trichlorophosphate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2005.07.140

Reference yield:

: 868846-53-1
N-allyl-N-[2-(1H-indol-3-yl)-ethyl]-formaminde

: 868847-11-4
2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaH / tetrahydrofuran / 0 - 20 °C

2: POCl₃ / CH₂Cl₂ / 16 h / 0 °C

3: 0.78 g / tetrahydrofuran / -20 - 20 °C

With sodium hydride; trichlorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2005.07.140

Reference yield:

: 869096-24-2
9-tolylsulfonyl-4,9-dihydro-3H-β-carboline

: 868847-11-4
2-allyl-1-prop-1-ynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / tetrahydrofuran / 20 °C

2: 83 percent / NaH / tetrahydrofuran / 0 - 20 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.07.140