Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

Base Information

Chemical Name:Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride
CAS No.:75830-08-9
Molecular Formula:C₂₁H₂₅N₃O₅*ClH
Molecular Weight:435.908
Hs Code.:

Synonyms:Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

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Chemical Property of Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

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Technology Process of Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

There total 7 articles about Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75830-36-3
N-<(tert-butoxycarbonyl)-L-valinyl>-N-benzyl-N-(2-acetoxy-5-nitrobenzyl)amide

: 75830-08-9
Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 2 ℃; for 0.5h;
DOI:10.1021/jo00316a003

Reference yield:

: 53848-16-1
5-nitrosalicylaldehyde benzylamine Schiff base

: 75830-08-9
Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄, HCl

2: sodium hydroxide / H₂O

3: N-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 24 h / 25 °C

4: 80 percent / pyridine / 24 h / 2 °C

5: 0.082 g / HCl / dioxane / 0.5 h / 2 °C

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00316a003

Reference yield:

: 75830-37-4
N-(2-hydroxy-5-nitrobenzyl)benzylamine*HCl

: 75830-08-9
Acetic acid 2-{[(2-amino-3-methyl-butyryl)-benzyl-amino]-methyl}-4-nitro-phenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / H₂O

2: N-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide / 24 h / 25 °C

3: 80 percent / pyridine / 24 h / 2 °C

4: 0.082 g / HCl / dioxane / 0.5 h / 2 °C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00316a003